Trace Analysis - 1st Edition - ISBN: 9780126821024, 9781483264042

Trace Analysis

1st Edition

Volume 2

Editors: James F. Lawrence
eBook ISBN: 9781483264042
Imprint: Academic Press
Published Date: 28th December 1982
Page Count: 286
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Description

Trace Analysis, Volume 2 is devoted to critical discussions of selected topics in organic and inorganic analytical chemistry including instrumentation, techniques, and applications to the detection, identification, and quantitation of trace quantities of substances in a large variety of sample materials. The volume presents expositions of selected topics on trace analysis such as vitamin analysis in foods and tissues; liquid chromatography - mass spectrometry with emphasis on approaches to interfacing; approaches to the isolation and concentration of trace organics from aqueous samples; and the advantages of unmodified silica gel for the chromatographic separation of polar substances. The book will be highly useful to both organic and inorganic chemists.

Table of Contents


Contents

Contributors

Preface

Contents of Volume 1

Trace Analysis of Vitamins by Liquid Chromatography

I. Introduction

II. Fat-Soluble Vitamins

III. Water-Soluble Vitamins

IV Conclusion

References

Combining Liquid Chromatography with Mass Spectrometry

I. Introduction

II. The Mass Spectrometer as a Detector for Liquid Chromatography

III. Off-Line Techniques

IV. On-Line Techniques

V. Alternative Methods of Vaporization and Ionization with Possible Applications to LC-MS

VI. Applications and Conclusions

References

Applications of Steric Exclusion Chromatography in Trace Analysis

I. Introduction

II. Basics of SEC

III. Advantages of the SEC Technique

IV. Disadvantages of the SEC Technique

V. Recent Advances in SEC Columns

VI. Utility of SEC in Trace Analysis

VII. Approaches for Use of SEC in Trace Analysis

VIII. Off-Line Multidimensional SEC Techniques

IX. On-Line Multidimensional SEC Techniques

X. Problems and Troubleshooting

References

Trace-Enrichment Techniques for Organic Trace Analysis

I. Trace Enrichment: Definition

II. Environmental Applications

III. Clinical Applications

IV. Pharmacological Applications

References

HPLC Analysis of Polar Substances on Unmodified Silica

I. Introduction

II. Literature Survey

III. Nonaqueous Systems Containing Aliphatic Carboxylic Acids

IV. Nonaqueous Systems Containing Amines

V. Coordinating Amine- and Carboxylic Acid-Based Separations for Optimum Resolution of Complex Samples

VI. Conclusions

References

Index


Details

No. of pages:
286
Language:
English
Copyright:
© Academic Press 1982
Published:
Imprint:
Academic Press
eBook ISBN:
9781483264042

About the Editor

James F. Lawrence

Ratings and Reviews