Semimicro Quantitative Organic Analysis focuses on the analytical phase of research and chemistry of natural products, as well as analysis of gases and methods used in identifying iodine and other substances.
The manuscript first offers information on the determination of carbon, hydrogen, and nitrogen, and the use of Kjeldahl and Dumas methods in the determination of nitrogen. The book also ponders on the determination of halogens, including the use of ethanolamine-sodium, Carius, and sodium peroxide fusion methods and the Liepert volumetric method for iodine.
The publication discusses the determination of sulfur and phosphorus, as well as the alkali-nitrate fusion method for converting organic phosphorus to orthophosphate and Woy's procedure for weighing phosphorus as phosphomolybdic anhydride. The text also reviews the determination of methoxyl and ethoxyl and acetyl groups; determination of neutralization equivalent and molecular weights; and determination of volatile fatty acids.
The manuscript is a dependable reference for readers interested in the chemistry of natural products.
Contents I. Introduction II. The Determination of Carbon and Hydrogen III. The Determination of Nitrogen by the Kjeldahl Method IV. The Dumas Method for the Determination of Nitrogen V. The Determination of Halogens VI. The Determination of Sulfur VII. The Determination of Phosphorus VIII. The Determination of Methoxyl and Ethoxyl Groups IX. The Determination of Acetyl Groups X. The Determination of the Neutralization Equivalent XI. The Determination of Molecular Weights XII. The Determination of Volatile Fatty Acids XIII. Some Useful Tables Table XII, Gravimetric Factors Table XIII, Barometric Corrections for Temperature Table XIV, Atomic and Molecular Formulas and Some of Their Multiples Table XV, The Carbon and Hydrogen Percentage and Molecular Weights of A Series of CHO Compounds From C15 To C32 Table XVI, 5-Place Logarithm Table Index
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- © Academic Press 2043
- 1st January 1943
- Academic Press
- eBook ISBN: