Determination of Organic Structures by Physical Methods V4

Determination of Organic Structures by Physical Methods V4

1st Edition - January 28, 1971

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  • Editor: F.C. Nachod
  • eBook ISBN: 9780323152341

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Description

Determination of Organic Structures by Physical Methods, Volume 4 is a seven-chapter text that discusses the refinements of some established physical methods for organic structure determination. Each chapter of this book examines specific physical method, including high-field and pulsed NMR, nuclear magnetic double resonance spectroscopy, and 15N, 13C, and 31P nuclear magnetic resonance. The historical developments, principles, instrumentation, and applications to organic chemistry of these methods are discussed. This work will be of value to organic and analytical chemists and researchers.

Table of Contents


  • List of Contributors

    Preface

    Contents of Other Volumes

    1. Applications of High-Field NMR Spectroscopy

    I. Introduction

    II. High-Field Spectrometers

    III. Structure Determinations

    IV. Small Molecules

    V. Polymers

    References

    2. Pulsed NMR Methods

    I. Introduction

    II. Theory of the Pulsed NMR Experiment

    III. Fourier Transform Spectroscopy

    IV. Spin-Echo Experiments in Liquids

    V. Spin-Echo Experiments in Solids

    VI. Spin-Lattice Relaxation Methods

    References

    3. Nuclear Magnetic Double Resonance Spectroscopy

    I. Introduction

    II. Nomenclature

    III. Basic Theoretical Considerations

    IV. Experimental Aspects

    V. Chemical Applications

    References

    4. 15N Nuclear Magnetic Resonance

    I. Introduction and Scope

    II. Experimental Techniques

    III. Theory

    IV. Results

    V. The Future

    References

    5. NMR Spectra of the Heavier Elements

    I. Introduction

    II. Experimental Techniques

    III. Chemical Shift Measurements

    IV. Coupling Constant Correlations

    V. Conclusions

    References

    6. 13C Nuclear Magnetic Resonance

    I. Introduction

    II. Techniques and Methods of Assignment

    III. Chemical Shifts

    IV. Coupling Constants

    V. Applications

    Appendix

    References

    7. 31P Nuclear Magnetic Resonance

    I. Introduction

    II. Phosphorus-31 Chemical Shifts

    III. Coupling with Other Magnetically Active Nuclei

    IV. Practical Usage of 31P NMR

    References

    Author Index

    Subject Index




Product details

  • No. of pages: 396
  • Language: English
  • Copyright: © Academic Press 1971
  • Published: January 28, 1971
  • Imprint: Academic Press
  • eBook ISBN: 9780323152341

About the Editor

F.C. Nachod

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