
Applications in High Resolution Mass Spectrometry
Food Safety and Pesticide Residue Analysis
Description
Key Features
- Arms researchers with an in-depth resource devoted to the rapid advances in HRMS tools and strategies for pesticide residue analysis in food
- Provides a complete overview of analytical methodologies and applications of HRMS, including UHPLC-HRMS, HRMS coupled with time of flight (TOF) and/or GC-Orbitrap, and flow injection-HRMS
- Discusses the current international regulations and legislation related to the use of HRMS in pesticide residue analysis
- Features a chapter on the hardware and software available for HRMS implementation
- Offers separate chapters on HRMS applied to pesticide residue analysis in fruits and vegetables and in food from animal origin
Readership
Researchers in universities, government agencies, and private industry in food safety, food chemistry, analytical chemistry, and toxicology; and graduate students in these areas
Table of Contents
Chapter 1. HRMS: Fundamentals and Basic Concepts
- 1.1. Introduction (To High-Resolution Mass Spectrometry)
- 1.2. Resolution and Mass Resolving Power
- 1.3. Accurate Mass Measurement: Exact Mass and Mass Defect
- 1.4. Mass Calibration in High-Resolution Mass Spectrometry
- 1.5. General Considerations
Chapter 2. HRMS: Hardware and Software
- 2.1. Introduction
- 2.2. Principles of High-Resolution Mass Spectrometry Analyzers
- 2.3. Time-of-Flight Mass Spectrometry: Instrument Configuration and Main Features
- 2.4. Orbitrap Analyzers: Instrument Configurations and Main Features
- 2.5. Acquisition Modes in High-Resolution Mass Spectrometry
- 2.6. Databases and the Internet Resources for High-Resolution Mass Spectrometry
Chapter 3. Analytical Strategies Used in HRMS
- 3.1. Introduction
- 3.2. Advantages of High-Resolution Mass Spectrometry in Pesticide Analysis
- 3.3. Data Analysis Workflows in High-Resolution Mass Spectrometry
- 3.4. Conclusions
Chapter 4. Current Legislation on Pesticides
- 4.1. Introduction
- 4.2. Pesticides
- 4.3. Legislation
- 4.4. Analytical Quality Control—Method Validation
- 4.5. Mass Spectrometry in Pesticide Residue Analysis
Chapter 5. Advanced Sample Preparation Techniques for Pesticide Residues Determination by HRMS Analysis
- 5.1. Introduction
- 5.2. Matrix Effects and the Influence of Coextracted Components
- 5.3. Sample Preparation Techniques for Pesticide Residue Determination by Chromatographic Techniques Coupled to High-Resolution Mass Spectrometry
- 5.4. Perspectives and Conclusions
Chapter 6. Applications of Liquid Chromatography Coupled With High-Resolution Mass Spectrometry for Pesticide Residue Analysis in Fruit and Vegetable Matrices
- 6.1. Introduction
- 6.2. Applications of Pesticide Residue Analysis in Fruit and Vegetable Samples by LC-HRMS
- 6.3. Optimized Sample Preparation and Chromatographic Conditions for Mass Analyzers
- 6.4. Analytical Method Validation
- 6.5. Accurate Measurement of Pesticide Residues in Fruit and Vegetable Samples
- 6.6. Evaluation of Pesticide Residues in Fruit and Vegetable Samples
- 6.7. Conclusion
Chapter 7. Application of HRMS in Pesticide Residue Analysis in Food From Animal Origin
- 7.1. Introduction
- 7.2. Instrumental Requirements
- 7.3. Analytical Procedures: Extraction and Chromatographic Conditions
- 7.4. Quantitative and Qualitative Applications
- 7.5. Differences Between Low-Resolution Mass Spectrometry and High-Resolution Mass Spectrometry Analytical Methods
- 7.6. Overview and Future Perspectives
Chapter 8. Recent Advances in HRMS Analysis of Pesticide Residues Using Atmospheric Pressure Gas Chromatography and Ion Mobility
- 8.1. Introduction
- 8.2. Atmospheric Pressure Gas Chromatography
- 8.3. Time-of-Flight Mass Spectrometry
- 8.4. Ion Mobility Separation
- 8.5. Summary and Conclusion
Chapter 9. Direct Analysis of Pesticides by Stand-Alone Mass Spectrometry: Flow Injection and Ambient Ionization
- 9.1. Introduction
- 9.2. Flow Injection Analysis
- 9.3. Ambient Mass Spectrometry
- 9.4. Final Remarks and Future Trends
Chapter 10. Identification of Pesticide Transformation Products in Food Applying High-Resolution Mass Spectrometry
- 10.1. Introduction
- 10.2. Experimental
- 10.3. Imidacloprid Metabolites in Plants
- 10.4. Imazalil Metabolites in Plants and Soil
- 10.5. Propiconazole Metabolites in Plants and Soil
- 10.6. Conclusions
Product details
- No. of pages: 360
- Language: English
- Copyright: © Elsevier 2017
- Published: March 7, 2017
- Imprint: Elsevier
- Paperback ISBN: 9780128094648
- eBook ISBN: 9780128096482
About the Editors
Roberto Romero-González
Affiliations and Expertise
Antonia Frenich
Affiliations and Expertise
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