Sample Preparation for Trace Element Analysis
- Zoltan Mester, Institute for National Measurement Standards, National Research Council, Ottawa, Canada
- Ralph Sturgeon, Institute for National Measurement Standards, National Research Council, Ottawa, Canada
Anyone required to undertakes trace metal analysis, including those in academic chemistry, geoscience and food science departments, federal regulatory agencies such as the FDA and EPA, as well as national bodies associated with geology, agriculture, etc. Additionally, contract environmental based laboratories and various industries such as food, oil and microelectronics.
- Published: December 2003
- Imprint: ELSEVIER
- ISBN: 978-0-444-51101-0
"In summary, this book provides valuable information and means a vast effort to cope with modern sample preparation techniques for trace element analysis and speciation. The wide scope covered makes it recommendable to academics, routine, laboratories and organisation dealing with trace element analysis. There is no doubt that the editors have achieved a leading book in this field for many years to come."
Carlos Bendicho, University of Vigo, Spain, SPECTROCHIMICA ACTA, PART B, Vol.59, 2004
"In conclusion, this book gives an extensive review of sample-preparation techniques that can be used for trace-element determination, with specific applications in some case studies. In addition, most chapters give an extensive, recent bibliography on the subject. Despite its broad coverage, it is well organised, and it would be very useful for scientists working in that field, especially as there are numerous detailed applications."
Douglas N. Rutledge, Paris, France, TRENDS IN ANALYTICAL CHEMISTRY, Vol. 23, No. 5, 2004
Table of Contents1. Sampling and Sample Preservation for Trace Element Analysis (B.G. Kratochvil).
2. Sources of Analyte Contamination and Loss during the Analytical Process (P. Schramel, G. Knapp.
3. Calibration approaches for trace element determination (D.C. Baxter, I. Rodushkin).
4. Stated references for ensuring traceability of trace element analysis (Ph. Quevauviller).
5. Detection Methods for the Quantitation of Trace Elements (L. Ebdon et al.).
Digestion and extraction approaches.
6. Wet digestion methods (H. Matusiewicz).
7. Dry ashing (M. Hoenig).
8 Microwave based extraction (E.E. King, D. Barclay).
9. Fusion and fluxes (F. Claisse).10. Supercritical fluid extraction (J.M. Bayona et al.).
11. Accelerated Solvent Extraction of Organometallic and Inorganic Compounds (J. Ezzell).
12. Sonication as sample preparation method for elemental analysis (K. Ashley).
13. Solid Phase Microextraction as a Tool for Trace Element determination (Z. Mester, R. Sturgeon).
14. Solid phase extraction (V. Camel).
15. Chelation solvent extraction for separation of metal ions (Taketoshi Nakahara, Hideyuki Itabashi).
16. Cryogenic trapping for speciation analysis (O.F.X. Donard et al.).
17. Biotrapping as an alternative to metal preconcentration and speciation (C. Camara, Y. Madrid).
18. Membrane extraction (Jan &Åring;ke J&öuml;nsson, L. Mathiasson).
19. Derivatization and Vapor Generation Methods for Trace Element Analysis and Speciation (Yong Cai).
20. Laser ablation sampling (R.E Russo, D.P. Baldwin).
21. Flow injection techniques for sample pretreatment (Zhao-Lun Fang).
22. Automation of sample preparation (M.D. Luque de Castro, J.L. Luque Garc&íacute;a).
23. Sample Preparation for Crude Oil, Petroleum Products and Polymers (R.I. Botto).
24. Sample preparation of geological samples, soils and sediments (P.J. Potts, P. Robinson).
25. Sample preparation for food analysis (M. Ihnat).
26. The Determination of Trace Elements in Water (S. Willie).
27. Aerosol sampling and sample preparation for elemental analysis (J. Hlavay).
28. Sample preparation for industrial waste analysis (R. Clement, P. Drouin).
29. Sample preparation for semiconductor materials(Katsu Kawabata et al.).
Trace element speciation
30. Sampling and sample treatment in the analysis of organotin compounds in environmental samples (R. Morabito).
31. Sample preparation for arsenic speciation(W. Goessler, D. Kuehnelt).
32. Sample preparation for speciation of selenium(J.A. Caruso et al.).
33. Sample preparation for mercury speciation (H. Hintelmann).
34. Sample preparation for speciation of lead(F.C. Adams, M. Heisterkamp).
35. Sample preparation for chromium speciation (M.De La Guardia, A. Morales-Rubio).
36. Sample preparation for metal-based drugs (R. Barefoot).
37. Sample preparation for speciation analysis for metallobiomolecules (R. Lobinski et al.).
38. Sample preparation for the analysis of volatile metal species (J. Feldmann).
39. Sequential extraction (G. Rauret, A. Sahuquillo).