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| GAS CHROMATOGRAPHY AND MASS SPECTROMETRY
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A Practical Guide
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By
Fulton Kitson
Barbara Larsen
Charles McEwen
Description
This guide provides, under one cover, a wealth of practical information designed to facilitate the effectiveness of the GC/MS user. Separation
conditions for numerous compound types are provided along with derivatized and underivatized compounds. A section on how to interpret
mass spectral data, an extensive correlation of ion masses and neutral losses with possible structures, and examples of mass spectra
are provided to further aid structure determination. Also included are basic information on instrumentation, ionization methods, quantitation,
tips on the operation of mass spectrometers, the best derivatization procedures for a variety of compound types, troubleshooting techniques,
and a variety of other information found to be useful to the practicing user of GC/MS instrumentation. This guide would be immediately
valuable to the novice as well as the experienced GC/MS user who may not have the breadth of experience covered in this book.
Audience
Researchers, students, and technicians in biochemistry, biotechnology, protein science, and many areas of biological, biomedical, and
medical research will be interested. Also interesting to an international audience for use as a handbook and text reference.
Contents
Preface.
Part I: The Fundamentals of GC/MS:
What Is GC/MS.
Mass Spectral Interpretation.
Quantitation.
Additional Literature
Pertaining to Part I.
Part II: GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types:
Acids.
Alcohols.
Aldehydes.
Amides.
Amines.
Amino Acids.
Common Contaminants.
Drugs and Metabolites.
Esters.
Ethers.
Fluorinated Compounds.
Gases.
Glycols.
Halogenated Compounds.
Hydrocarbons.
Isocyanates.
Ketones.
Nitriles.
Nitroaromatics.
Nitrogen-Containing Hetrocyclics.
Nucleosides.
Pesticides.
Phenols.
Phosphorus Compounds.
Plasticizers.
Prostaglandins.
Solvents and Impurities.
Steriods.
Sugars.
Sulfur
Compounds.
Additional Literature Pertaining to Part II.
Part III: Ions for Determining Unknown Structures:
M – 1 to
M ?200.
Part IV: Appendices:
Definitions of Terms Related to Gas Chromatography.
Tips for Gas Chromatography.
Derivatives
Found Useful in GC/MS.
Cross Index Chart for GC Phases.
McReynolds' Constants.
Simple GC Troubleshooting.
Definitions of Terms Related
to Mass Spectrometry.
Tips and Troubleshooting for Mass Spectrometry.
Atomic Masses and Isotope Abundances.
Structurally Significant
McLafferty Rearrangement Ions.
Isotope Patterns for ClxBry.
Mixtures for Determining Mass Spectral Resolution.
Additional Literature
Pertaining to Part IV.
Index.
| Bibliographic details |
Paperback, 381 pages, publication date: AUG-1996
ISBN-13: 978-0-12-483385-2
ISBN-10: 0-12-483385-3
Imprint: ACADEMIC PRESS
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| Price and Ordering |
Price:
EUR 85.95
USD 115
GBP 73
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Last update: 4 Sep 2009
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