Thermal Analysis V2

Thermal Analysis V2

Inorganic Materials and Physical Chemistry

1st Edition - January 1, 1969

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  • Editor: Robert F. Jr. Schwenker
  • eBook ISBN: 9780323142267

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Description

Thermal Analysis, Volume 2: Inorganic Materials and Physical Chemistry covers the proceedings of the Second International Conference on Thermal Analysis, held in Holy Cross College, Worcester, Massachusetts on August 18-23, 1968. This symposium surveys the various methods and applications of thermal analysis, as well as the distribution of various aspects of thermal analysis in different countries. This book is organized into four sections encompassing 51 chapters, and begins with discussion on the application of differential thermal analysis to metallurgical inorganic materials and reactions for industrial process optimization. These topics are followed by a consideration of other techniques, such as X-ray methods and thermography. The Physical Chemistry part highlights the reaction kinetics and thermodynamics of various chemical reactions, including oxidation and polymerization, using thermogravimetry and calorimetry techniques. The following part focuses on mineral analysis using combined techniques of thermoanalytic-mass spectrometry and differential thermal analysis-thermogravimetry. The last part deals with the application of thermal analysis in applied sciences.

Table of Contents


  • Contents of Volume 1

    Contributors

    Foreword

    Preface

    Section 3. Inorganic Materials and Metallurgy

    Differential Thermal Analysis of Boric Acid, Boric Oxide, and Potassium Fluoborate

    The Pyrosynthesis of Alkaline Earth Zincates

    Thermal Analysis of Promethium Oxalate

    The Thermal Decomposition of Potassium Oxalato Complexes of Nickel, Cobalt, and Copper

    DTA and X-Ray Analysis of "Rare Earth - Chalcogen" Systems

    Thermographic Study of the Structures of Some Simple, Mixed, and Binuclear Chelates of EDTA

    Thermography as a Method of Inorganic Synthesis

    A Thermoanalytical Study of the Effects of Various Fluorides on the Reaction between Potassium Chlorate and Magnesium

    Application of Differential Thermal Analysis to the Study of Phase Equilibria in Metal Systems

    Use of DTA for the Determination of the Monoclinic-Tetragonal Transformation in Zirconia and Zirconia-based Systems

    Studies on Thermal Analysis of the Vanadates of Tin and Silver, and Chemisorption of Oxygen and Hydrogen on these Vanadates as Catalysts

    The Influence of Oxide Additions on the Reduction of UO3 and U3O8 as Measured by DTA and TG

    Thermal Oxidation of Nickel Silicon Alloy

    Studies on Thermal Analysis of the Vanadates of Copper, Lead, and Cobalt

    Relative Thermal Stabilities of Copper (II) Sulfate Pentahydrate and Barium Chloride Dihydrate Compared to Their Deuterium Oxide Analogs

    The Thermal Decomposition of EuFe(CN)6•5H2O and NH4EuFe(CN)6•4H2O

    Thermal Analysis in Studies of Dehydration Processes

    Study of Dehydration of Magnesium Sulfate Heptahydrate

    Die Anwendung Thermographischer Methoden bei Hochtemperaturuntersuchungen an Oxidsystemen

    Section 4. Physical Chemistry

    The Simultaneous Determination of the Kinetics and Thermodynamics of Decomposition by Isothermal DTA

    Kinetics of the Reaction between MgSO4 and Cr2O3

    Surface Area Effects on the Oxidation Kinetics of Pyrolytic Graphite

    Note on the Algorithmisation of Kinetic Data Computation from Thermogravimetric Traces with Increasing Temperature

    Calculation of Activation Energy of Decomposition Reactions from Thermogravimetric Analysis

    Kinetic Investigation of Polymerization Reaction with Differential Scanning Calorimeter

    A Thermogravimetric Method Applied to the Study of Solid State Dehydration Kinetics in Vacuum

    Determination of the Activation Energy Change of CaCO3 under Influence of Various Environmental Gases

    The Historical Development of Applied Nonisothermal Kinetics

    A Contribution to the Kinetics and Mechanism of the Thermal Decomposition of Alkali Metal Picrates

    The Calorimetric Observation of Solid State Reactions in Aluminum Alloys

    Isothermal Preconditioning for Quantitative Thermal Analysis

    Application of Differential Thermal Analysis to the Quantitative Measurement of Enthalpy Changes

    The Reduction of Quantitative Differential Thermal Analysis Data to Basic Thermodynamic and Kinetic Quantities

    Decomposition Mechanism of Mg(OH)2 and Mg(OD)2I

    Section 5. Minerals

    Differential-Thermo Analyse von Gemischen aus Festen Brennstoffen mit Oxydationsmitteln und Inhibitoren

    Thermoanalytic-Mass Spectrometrical Investigation of an Oil Shale Containing Dawsonite

    The Gibbsite Dehydroxylation Fork

    Simultaneous DTA-TG-MSA Apparatus for Thermal Study of Natural Fuels

    Investigations on the Thermal Curves of Alunite Associated with Other Minerals

    Thermal Decomposition Rate of Molybdenite in Vacuum

    Section 6. Applied Sciences

    The Rapid Determination of Solid Fat Index with a Scanning Calorimeter

    DTA/TGA Investigation of Reactions in Sodium-Lead-Silicate Glass Batch

    Heat Transfer and Coal Pyrolysis

    The Use of Differential Thermal Analysis-Effluent Gas Analysis in Metallurgical Research Investigations

    The Identification and Estimation of Carbonaceous Materials by DTA

    A Study of Differential Thermal Analysis (DTA) - Effluent Gas Analysis (EGA) for the Determination of Planetary Environmental Parameters

    Differential Thermal Analysis Studies of Compound Semiconductors

    The Formation and Surface Properties of Electron Emissive Coatings I. Thermogravimetric and Gas Evolution Studies of Alkaline Earth Carbonates and Hydroxides

    TGA Measurement of Curie Temperature of Some Commercial Ferrites

    A Mass-Thermal Method for Studying Ablative Polymer Degradation Mechanisms

    The Impact of Thermal Analysis on Nuclear Ammonium Polyuranate Preparation

    Appendices

    1.Recommendations for Reporting Thermal Analysis Data

    2 Recommendations for Nomenclature in Thermal Analysis

    3 A Report from the Committee on Standardization International Confederation for Thermal Analysis

    Subject Index

Product details

  • No. of pages: 842
  • Language: English
  • Copyright: © Academic Press 1969
  • Published: January 1, 1969
  • Imprint: Academic Press
  • eBook ISBN: 9780323142267

About the Editor

Robert F. Jr. Schwenker

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