Preface. Contents. List of contributors. Selective pulses in NMR (S.J.F. Vincent, C. Zwahlen). Multiple selective excitation: a method to improve the efficiency of selective 1D and 2D experiments (P. Bigler). Concatenation of polarization transfer steps in 1D homonuclear chemical shift correlated experiments. Application to oligo- and polysaccharides (D. Uhrín). The selective reverse INEPT experiment (G.A. Morris, I.C. Clements). GROESY, gradient-enhanced selective 1D ROE measurements (P. Adell et al.). The DANTE-Z experiment (D. Canet, C. Roumestand). One-dimensional TOCSY and related 1D techniques (T.C. Wong). Use of high-power spin-lock purge pulses in high-resolution NMR spectroscopy (G. Otting). Decoupled HMBC (D-HMBC), an improved version of HMBC (H. Seto, K. Furihata). Optimal acquisition and presentation of HoMQC spectra (I. Pelczer, K.D. Bishop). High resolution diffusion ordered spectroscopy (G.A. Morris, H. Barjat). Chemical exchange measurements in NMR (A.D. Bain). Homonuclear two-dimensional cross-relaxation spectroscopy (N. Juranić et al.). Reference deconvolution (G.A. Morris, H. Barjat). The super fast inversion recovery (SUFIR) experiment (D. Canet et al.). Measurements of relaxation rates for low natural abundance I=1/2 nuclei (J. Kowalewski, L. Mäler).