Introduction to Quantitative Ultramicroanalysis - 1st Edition - ISBN: 9781483232003, 9781483270708

Introduction to Quantitative Ultramicroanalysis

1st Edition

Authors: I. M. Korenman
eBook ISBN: 9781483270708
Imprint: Academic Press
Published Date: 1st January 1965
Page Count: 244
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Introduction to Quantitative Ultramicroanalysis has been compiled on the basis of reports published by numerous authors. It does not claim to offer an exhaustive treatment of ultramicroanalysis, but it summarizes data on the subject and related experimental methods and techniques, newly designed requisite equipment, etc. Several procedures are described which have proved effective in analyzing minute amounts of sample. The weighing of extremely small objects is treated most extensively, as are the titration and colorimetry of solutions. The equipment used in ultramicroanalysis, in addition to its minute size, is of a highly specialized design. These unique features, as well as some of the simpler micromanipulators, are discussed in the related chapters.

Table of Contents

Foreword Chapter I. General Discussion

1. Classification of Analytical Techniques Based on the Amount of Substance Taken for Analysis 2. Ultramicroanalysis: Scope of Application 3. Ultramicroanalysis: Distinctive Features

Chapter II. Principal Techniques of Operation

1. Sampling Techniques 2. Addition and Measurement of Solutions 3. Reactions on Fibers, Paper and Gelatin 4. Microcrystalloscopic Tests 5. Reactions in Capillary Test Tubes and Cones 6. Tests in Sealed Capillaries 7. Reactions Involving the Use of Gaseous Reagents 8. Mixing and Shaking of Solutions 9. The Heating, Evaporating and Igniting Procedures 10. Isolating a Precipitate from Solution 11. the Washing of Vessels 12. Electrolysis 13. Extraction 14. Chromatography 15. Microscopic Determination of Size

Chapter III. Gravimetric Analysis

1. Balances and Weighing Procedures 2. Balances Using Thread Displacement 3. Balances Based on Torsion 4. Helical (Spring) Balances 5. Weighing Pans and Loops 6. Balance Calibration 7. Weighing Errors 8. Gravimetric Determinations 9. Dry Residue Determination 10. Ash Determination 11. Lead, Silver and Mercury Determination 12. Determination of Relative Density of Liquids 13. Density Determination of Solids

Chapter IV. Volumetric Analysis

1. Volumetric Analysis: Equipment and Techniques 2. Mercury-Seal Burettes 3. Air-Seal Burettes 4. Hydrostatic Burettes 5. Uncalibrated Burettes 6. Pipettes 7. Volumetric Flasks 8. Titration Vessels 9. Calibrating Measuring Instruments A. Burettes B. Pipettes 10. Errors of Titration A. Reading Errors B. Wetting and Overflow Errors C. Indicator Errors 11. Volumetric Determinations A. Determining the Normality of Worki


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© Academic Press 1965
Academic Press
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About the Author

I. M. Korenman

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