Inorganic Species, Part 3

Inorganic Species, Part 3

1st Edition - October 26, 1984

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  • Editor: Roger Minear
  • eBook ISBN: 9780323149280

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Description

Water Analysis, Volume III: Organic Species is a seven-chapter text that emphasizes the methods used for the determination and analysis of organic constituents in both natural and polluted waters. Chapters 1 and 2 deal with waste strength and waste pollution parameters of a nonspecific variety, such as biochemical oxygen demand, chemical oxygen demand, total organic carbon, spectroscopic measurements, electrochemical methods, and a number of other techniques that provide chemical class determinations. Chapter 3 provides the current methods for isolating, concentrating, and partitioning organic constituents from water. Chapter 4 examines gas chromatographic separations and analyses and capillary and packed-column techniques. This chapter also presents injector techniques, derivatizations, detector types, qualitative and quantitative analyses, and a representative list of applications. Chapter 5 discusses the principles of organic mass spectrometry, mass analysis, ion detection, chromatography/mass spectrometry, tandem mass spectrometry, qualitative and quantitative analysis, and selected applications. Chapter 6 describes the principles and applications of using high performance liquid chromatography for water analyses, as well as the necessary equipment, the chromatographic process, and practical use and optimization of the method. Chapter 7 covers the use of infrared spectrophotometry for analyzing for organic pollutants in water, considering both theoretical aspects and practical applications of this technique.

Table of Contents


  • List of Contributors

    Preface

    1 Waste Strength and Water Pollution Parameters

    I. Introduction

    II. Oxygen Demand as a Pollution Control Parameter

    III. Mathematical Modeling of the BOD Reaction

    IV. BOD Test Methods

    V. Factors Affecting BOD Measurement

    VI. Accuracy and Precision of BOD Tests

    References

    2 Chemical Nonspecific Organics Analysis

    I. Introduction

    II. Elemental Parameters

    III. Oxygen Demand

    IV. Spectrophotometric Methods

    V. Electrochemical Methods

    VI. Class Determinations

    VII. On-Line Monitors

    VIII. Comparison of Nonspecific Parameters

    References

    3 Concentration, Partitioning, and Isolation Techniques

    I. Introduction

    II. Equipment and Reagent Selection and Cleanup

    III. Techniques for Volatiles

    IV. Techniques for Semivolatiles

    V. Techniques for Low Molecular Weight Nonvolatiles

    VI. Techniques for High Molecular Weight Constituents

    VII. Comprehensive Analytical Schemes

    VIII. Summary

    References

    4 Gas Chromatography

    I. Introduction

    II. Gas Chromatographic Techniques and Equipment

    III. Applications

    References

    5 Organic Mass Spectrometry

    I. Introduction

    II. Principles of Organic Mass Spectrometry

    III. Mass Analysis

    IV. Ion Detection

    V. Chromatography/Mass Spectrometry

    VI. Tandem Mass Spectrometry

    VII. Qualitative Analysis

    VIII. Quantitative Analysis

    IX. Selected Applications

    References

    6 The Use of HPLC for Water Analysis

    I. Introduction

    II. Equipment for HPLC

    III. Detectors for HPLC

    IV. Description of the Chromatographic Process

    V. Solute Retention in HPLC

    VI. Making a Separation

    VII. Optimizing the Separation

    References

    7 Infrared Spectrophotometry of Pollutants in Water Systems

    I. Introduction

    II. Recording of Infrared Spectra

    III. Theoretical Considerations

    IV. Fundamentals of Spectral Interpretations

    V. Spectral Interpretations

    VI. Infrared Techniques

    VII. Pesticide Analysis

    VIII. Phenol Analysis

    IX. Petroleum Analysis

    X. Petroleum Identification

    XI. Characterization and Identification of Spilled Petroleum Oils

    XII. Linear Discriminant Function Analysis

    XIII. Fourier Transform Infrared Spectroscopy

    References

    Index




Product details

  • No. of pages: 468
  • Language: English
  • Copyright: © Academic Press 1984
  • Published: October 26, 1984
  • Imprint: Academic Press
  • eBook ISBN: 9780323149280

About the Editor

Roger Minear

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