Gravimetric Analysis

International Series of Monographs in Analytical Chemistry, Vol. 7

1st Edition - January 1, 1965
Author: László Erdey
Editors: R. Belcher, L. Gordon
Language: English
eBook ISBN:
9 7 8 - 1 - 4 8 3 2 - 2 2 5 9 - 2

Gravimetric Analysis, Part III describes the experimental procedures for the gravimetric analysis of various compounds. This book is composed of 13 chapters that also present… Read more

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Gravimetric Analysis, Part III describes the experimental procedures for the gravimetric analysis of various compounds. This book is composed of 13 chapters that also present sample preparation protocols. The first four chapters survey the steps for halogen compound determination. The succeeding chapters provide the procedures for gravimetric determination of cyanide, thiocyanate ions, sulfur, nitrogen, phosphorus, carbon, silicon, and boron. The final chapter considers other aspects of gravimetric experiments, including apparatus cleaning, reagents, and numerical calculation of the result. This book will prove useful to analytical and inorganic chemists, teachers, and students in the allied fields.

48. Chlorine 48.1. Digestion of Organic Halogen-Containing Substances 48.2. Determination of Chloride in the Form of Silver Chloride 48.3. Determination of Perchlorate Ions in the Form of Potassium Perchlorate 48.4â€”48.5. Separation Methods References49. Bromine 49.1. Determination of Bromide in the Form of Silver Bromide 49.2â€”49.3. Separation Methods References50. Iodine 50.1. Determination of Iodide in the Form of Silver Iodide 50.2. Determination of Iodide in the Form of Palladium(II) Iodide 50.3â€”50.5. Separation Methods References51. Fluorine 51.1. Determination in the Form of Calcium Fluoride 51.2. Determination in the Form of Lead Chlorofluoride 51.3â€”51.5. Separation Methods References52. Cyanide 52.1. Determination in the Form of Silver Cyanide 52.2. Determination of Cyanide in Mercury(II) Cyanide 52.3â€”52.4. Separation Methods References53. Thiocyanate Ions 53.1. Determination in the Form of Silver Thiocyanate 53.2. Determination in the Form of Copper(I) Thiocyanate 53.3. Determination in the Form of Barium Sulphate 53.4â€”53.7. Separation Methods References54. Sulfur 54.1. Determination of Sulphate Ions 54.2. Determination of Sulphide Ions 54.3. Determination of the Sulfur Content of Non-volatile Organic Substances 54.4. Determination of the Sulfur Content of Volatile Organic Substances (Petrol). Lamp Sulfur 54.5. Determination of the Total Sulfur Content of Gases 54.6. Determination of the Sulfur Content of Coal 54.7. Digestion of Organic Substances Containing Sulfur with Red Fuming Nitric Acid in a Bomb 54.8. Determination of the Sulfur Content of Non-volatile Organic Substances by Combustion in a Bomb (Bomb Sulfur) 54.9. Determination of the Sulfur Content of Organic Substances after Decomposition in a Parr Bomb 54.10. Determination of Sulfite, Dithionite, Thiosulfate and Peroxydisulfate Ions 54.11. Separation of Sulfite and Thiosulfate 54.12. Simultaneous Determination of Sulfide, Sulfite and Thiosulfate 54.13. Determination of Elementary Sulfur References55. Nitrogen 55.1. Determination in the Form of Nitron Nitrate References56. Phosphorous 56.1. Determination of Phosphate Ions 56.2. Determination of Pyrophosphate Ions 56.3. Determination of Phosphite Ions 56.4. Determination of Hypophosphite Ions 56.5. Determination of Hypophosphate Ions 56.6â€”56.26. Separation of Phosphorus Compounds References57. Carbon 57.1. Determination of Carbon and Hydrogen in Organic Substances by Combustion 57.2. Determination of Carbonates 57.3. Determination of the Carbon Content of Iron and Steel58. Silicon 58.1. Precipitation and Dehydration of Silicic Acid 58.2. Determination of the Silicic Acid Content of Silicates 58.3. Determination of Oxides Accompanying silicic Acid 58.4. Determination of Silicic Acid in the Form of the Quinoline Salt of Silicomolybdic Acid References59. Boron 59.1. Separation of Boric Acid by Distillation. Gravimetric Determination in the Form of Calcium Borate References60. Appendix 60.1. Cleaning of Vessels Used in Analysis 60.2. Chemicals Used in Analysis 60.3. Gases Used for Analysis 60.4. Concentration of Reagents and Solutions to be Analyzed 60.5. Numerical Calculation of the ResultLiteratureTablesAuthor IndexSubject Other Titles in the Series