Gravimetric Analysis

Gravimetric Analysis

International Series of Monographs in Analytical Chemistry, Vol. 7

1st Edition - January 1, 1965

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  • Author: László Erdey
  • eBook ISBN: 9781483222592

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Gravimetric Analysis, Part III describes the experimental procedures for the gravimetric analysis of various compounds. This book is composed of 13 chapters that also present sample preparation protocols. The first four chapters survey the steps for halogen compound determination. The succeeding chapters provide the procedures for gravimetric determination of cyanide, thiocyanate ions, sulfur, nitrogen, phosphorus, carbon, silicon, and boron. The final chapter considers other aspects of gravimetric experiments, including apparatus cleaning, reagents, and numerical calculation of the result. This book will prove useful to analytical and inorganic chemists, teachers, and students in the allied fields.

Table of Contents

  • 48. Chlorine

    48.1. Digestion of Organic Halogen-Containing Substances

    48.2. Determination of Chloride in the Form of Silver Chloride

    48.3. Determination of Perchlorate Ions in the Form of Potassium Perchlorate

    48.4—48.5. Separation Methods


    49. Bromine

    49.1. Determination of Bromide in the Form of Silver Bromide

    49.2—49.3. Separation Methods


    50. Iodine

    50.1. Determination of Iodide in the Form of Silver Iodide

    50.2. Determination of Iodide in the Form of Palladium(II) Iodide

    50.3—50.5. Separation Methods


    51. Fluorine

    51.1. Determination in the Form of Calcium Fluoride

    51.2. Determination in the Form of Lead Chlorofluoride

    51.3—51.5. Separation Methods


    52. Cyanide

    52.1. Determination in the Form of Silver Cyanide

    52.2. Determination of Cyanide in Mercury(II) Cyanide

    52.3—52.4. Separation Methods


    53. Thiocyanate Ions

    53.1. Determination in the Form of Silver Thiocyanate

    53.2. Determination in the Form of Copper(I) Thiocyanate

    53.3. Determination in the Form of Barium Sulphate

    53.4—53.7. Separation Methods


    54. Sulfur

    54.1. Determination of Sulphate Ions

    54.2. Determination of Sulphide Ions

    54.3. Determination of the Sulfur Content of Non-volatile Organic Substances

    54.4. Determination of the Sulfur Content of Volatile Organic Substances (Petrol). Lamp Sulfur

    54.5. Determination of the Total Sulfur Content of Gases

    54.6. Determination of the Sulfur Content of Coal

    54.7. Digestion of Organic Substances Containing Sulfur with Red Fuming Nitric Acid in a Bomb

    54.8. Determination of the Sulfur Content of Non-volatile Organic Substances by Combustion in a Bomb (Bomb Sulfur)

    54.9. Determination of the Sulfur Content of Organic Substances after Decomposition in a Parr Bomb

    54.10. Determination of Sulfite, Dithionite, Thiosulfate and Peroxydisulfate Ions

    54.11. Separation of Sulfite and Thiosulfate

    54.12. Simultaneous Determination of Sulfide, Sulfite and Thiosulfate

    54.13. Determination of Elementary Sulfur


    55. Nitrogen

    55.1. Determination in the Form of Nitron Nitrate


    56. Phosphorous

    56.1. Determination of Phosphate Ions

    56.2. Determination of Pyrophosphate Ions

    56.3. Determination of Phosphite Ions

    56.4. Determination of Hypophosphite Ions

    56.5. Determination of Hypophosphate Ions

    56.6—56.26. Separation of Phosphorus Compounds


    57. Carbon

    57.1. Determination of Carbon and Hydrogen in Organic Substances by Combustion

    57.2. Determination of Carbonates

    57.3. Determination of the Carbon Content of Iron and Steel

    58. Silicon

    58.1. Precipitation and Dehydration of Silicic Acid

    58.2. Determination of the Silicic Acid Content of Silicates

    58.3. Determination of Oxides Accompanying silicic Acid

    58.4. Determination of Silicic Acid in the Form of the Quinoline Salt of Silicomolybdic Acid


    59. Boron

    59.1. Separation of Boric Acid by Distillation. Gravimetric Determination in the Form of Calcium Borate


    60. Appendix

    60.1. Cleaning of Vessels Used in Analysis

    60.2. Chemicals Used in Analysis

    60.3. Gases Used for Analysis

    60.4. Concentration of Reagents and Solutions to be Analyzed

    60.5. Numerical Calculation of the Result



    Author Index


    Other Titles in the Series

Product details

  • No. of pages: 312
  • Language: English
  • Copyright: © Pergamon 1965
  • Published: January 1, 1965
  • Imprint: Pergamon
  • eBook ISBN: 9781483222592

About the Author

László Erdey

About the Editors

R. Belcher

L. Gordon

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