Determination Of Organic Structures By Physical Methods V6 - 1st Edition - ISBN: 9780125134064, 9780323149204

Determination Of Organic Structures By Physical Methods V6

1st Edition

Editors: F.C. Nachod
eBook ISBN: 9780323149204
Imprint: Academic Press
Published Date: 28th January 1976
Page Count: 468
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Description

Determination of Organic Structures by Physical Methods, Volume 6 is a six-chapter text that describes the refinements of some established physical methods for organic structure determination. The opening chapters examine the application of mass spectroscopy to amino acid sequencing of oligopeptides and the computerized organic structure retrieval. The following chapters discuss the historical developments, principles, instrumentation, and application of flash photolysis and 29Si nuclear magnetic resonance to structure determination. A chapter considers the relevant theory from which information on internuclear distances can be obtained and the steady-state measurements, transient methods, as well as the use of Fourier transform technique. This chapter also explores the application of nuclear overhauser effect measurements to structural and stereochemical problems. The concluding chapter deals with the liquid crystal structure determination using NMR spectroscopy. This work will be of value to organic and analytical chemists and researchers.

Table of Contents


List of Contributors

Preface

Contents of Other Volumes

1. Amino Acid Sequencing of Oligopeptides by Mass Spectrometry

I. Introduction

II. Electron Impact Fragmentation of Derivatized Oligopeptides

III. Chemical Ionization of Derivatized and Underivatized Oligopeptides

IV. Field Desorption Ionization of Underivatized Oligopeptides

V. Derivatization Methods

VI. Analytical Techniques

VII. The Future of Mass Spectrometry for Peptide Sequencing

References

2. Computerized Structure Retrieval and Interpretation of Mass Spectra

I. Introduction

II. Inductive Approaches

III. Deductive Approaches

IV. The Combination Approaches

References

3. Flash Photolysis and Structure

I. Introduction

II. Instrumentation

III. Spectra of Free Radicals

IV. Electronic Structure of Excited States

V. Some Applications to Photobiological Systems

VI. Summary

References

4. 29Si Nuclear Magnetic Resonance

I. Introduction

II. 29Si Chemical Shifts

III. 29Si Spin-Spin Coupling Constants

IV. Relaxation and the Nuclear Overhauser Effect

References

5. The Nuclear Overhauser Effect

I. Introduction

II. Theory

III. Experimental Methods

IV. Chemical Applications

V. The Effects of Chemical Exchange and Internal Motion

References

6. Molecular Structures by NMR in Liquid Crystals

I. Introduction

II. The Liquid Crystals

III. Experimental Methods

IV. Spectral and Structural Analysis

V. Examples of Structural Determinations

Appendix

References

Author Index

Subject Index




Details

No. of pages:
468
Language:
English
Copyright:
© Academic Press 1976
Published:
Imprint:
Academic Press
eBook ISBN:
9780323149204

About the Editor

F.C. Nachod