Determination Of Organic Structures By Physical Methods V6
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Determination of Organic Structures by Physical Methods, Volume 6 is a six-chapter text that describes the refinements of some established physical methods for organic structure determination. The opening chapters examine the application of mass spectroscopy to amino acid sequencing of oligopeptides and the computerized organic structure retrieval. The following chapters discuss the historical developments, principles, instrumentation, and application of flash photolysis and 29Si nuclear magnetic resonance to structure determination. A chapter considers the relevant theory from which information on internuclear distances can be obtained and the steady-state measurements, transient methods, as well as the use of Fourier transform technique. This chapter also explores the application of nuclear overhauser effect measurements to structural and stereochemical problems. The concluding chapter deals with the liquid crystal structure determination using NMR spectroscopy. This work will be of value to organic and analytical chemists and researchers.
Table of Contents
List of Contributors
Preface
Contents of Other Volumes
1. Amino Acid Sequencing of Oligopeptides by Mass Spectrometry
I. Introduction
II. Electron Impact Fragmentation of Derivatized Oligopeptides
III. Chemical Ionization of Derivatized and Underivatized Oligopeptides
IV. Field Desorption Ionization of Underivatized Oligopeptides
V. Derivatization Methods
VI. Analytical Techniques
VII. The Future of Mass Spectrometry for Peptide Sequencing
References
2. Computerized Structure Retrieval and Interpretation of Mass Spectra
I. Introduction
II. Inductive Approaches
III. Deductive Approaches
IV. The Combination Approaches
References
3. Flash Photolysis and Structure
I. Introduction
II. Instrumentation
III. Spectra of Free Radicals
IV. Electronic Structure of Excited States
V. Some Applications to Photobiological Systems
VI. Summary
References
4. 29Si Nuclear Magnetic Resonance
I. Introduction
II. 29Si Chemical Shifts
III. 29Si Spin-Spin Coupling Constants
IV. Relaxation and the Nuclear Overhauser Effect
References
5. The Nuclear Overhauser Effect
I. Introduction
II. Theory
III. Experimental Methods
IV. Chemical Applications
V. The Effects of Chemical Exchange and Internal Motion
References
6. Molecular Structures by NMR in Liquid Crystals
I. Introduction
II. The Liquid Crystals
III. Experimental Methods
IV. Spectral and Structural Analysis
V. Examples of Structural Determinations
Appendix
References
Author Index
Subject Index
Product details
- No. of pages: 468
- Language: English
- Copyright: © Academic Press 1976
- Published: January 28, 1976
- Imprint: Academic Press
- eBook ISBN: 9780323149204
About the Editor
F.C. Nachod
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