Determination Of Organic Structures By Physical Methods V6

Determination Of Organic Structures By Physical Methods V6

1st Edition - January 28, 1976

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  • Editor: F.C. Nachod
  • eBook ISBN: 9780323149204

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Determination of Organic Structures by Physical Methods, Volume 6 is a six-chapter text that describes the refinements of some established physical methods for organic structure determination. The opening chapters examine the application of mass spectroscopy to amino acid sequencing of oligopeptides and the computerized organic structure retrieval. The following chapters discuss the historical developments, principles, instrumentation, and application of flash photolysis and 29Si nuclear magnetic resonance to structure determination. A chapter considers the relevant theory from which information on internuclear distances can be obtained and the steady-state measurements, transient methods, as well as the use of Fourier transform technique. This chapter also explores the application of nuclear overhauser effect measurements to structural and stereochemical problems. The concluding chapter deals with the liquid crystal structure determination using NMR spectroscopy. This work will be of value to organic and analytical chemists and researchers.

Table of Contents

  • List of Contributors


    Contents of Other Volumes

    1. Amino Acid Sequencing of Oligopeptides by Mass Spectrometry

    I. Introduction

    II. Electron Impact Fragmentation of Derivatized Oligopeptides

    III. Chemical Ionization of Derivatized and Underivatized Oligopeptides

    IV. Field Desorption Ionization of Underivatized Oligopeptides

    V. Derivatization Methods

    VI. Analytical Techniques

    VII. The Future of Mass Spectrometry for Peptide Sequencing


    2. Computerized Structure Retrieval and Interpretation of Mass Spectra

    I. Introduction

    II. Inductive Approaches

    III. Deductive Approaches

    IV. The Combination Approaches


    3. Flash Photolysis and Structure

    I. Introduction

    II. Instrumentation

    III. Spectra of Free Radicals

    IV. Electronic Structure of Excited States

    V. Some Applications to Photobiological Systems

    VI. Summary


    4. 29Si Nuclear Magnetic Resonance

    I. Introduction

    II. 29Si Chemical Shifts

    III. 29Si Spin-Spin Coupling Constants

    IV. Relaxation and the Nuclear Overhauser Effect


    5. The Nuclear Overhauser Effect

    I. Introduction

    II. Theory

    III. Experimental Methods

    IV. Chemical Applications

    V. The Effects of Chemical Exchange and Internal Motion


    6. Molecular Structures by NMR in Liquid Crystals

    I. Introduction

    II. The Liquid Crystals

    III. Experimental Methods

    IV. Spectral and Structural Analysis

    V. Examples of Structural Determinations



    Author Index

    Subject Index

Product details

  • No. of pages: 468
  • Language: English
  • Copyright: © Academic Press 1976
  • Published: January 28, 1976
  • Imprint: Academic Press
  • eBook ISBN: 9780323149204

About the Editor

F.C. Nachod

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