Table of Contents
- 1. Fundamental Relationships of Chromatography
Introduction. Retention. Flow in Porous Media. Band Broadening
Mechanism. Peak Shape Models. Parameters Affecting Resolution.
Optimization of Kinetic Column Variables. Principles of
Quantitation in Column Chromatography. References. 2. The
Column in Gas Chromatography Introduction. Packed Column
Gas-Liquid Chromatography. Open Tubular Columns. Evaluation of
the Quality of Open Tubular Columns. Retention in Gas-Liquid
Chromatography. Gas-Solid Chromatography. Preparative-Scale Gas
Chromatography. References. 3. Instrumental Aspects of Gas
Chromatography Introduction. Pneumatic Systems. Thermal
Zones. Sample Inlets. Detection Devices for Gas Chromatography.
Column Connectors and Effluent Splitters. References. 4 The
Column in Liquid Chromatography Introduction. Column Packing
Materials. Column Preparation. Column Evaluation and Test
Methods. Retention Mechanisms in Liquid Chromatography. Method
Development Strategies for Liquid Chromatography. Preparative-
Scale Liquid Chromatography. Capillary Electrophoretic Separation
Methods. References. 5. Instrumental Aspects of High Pressure
Liquid Chromatography Introduction. Requirements with Respect
to Extracolumn Dispersion. Solvent Reservoirs and Solvent
Degassing. Solvent Delivery Systems. Injection Devices.
Detectors. References. 6. Supercritical Fluid
Chromatography Introduction. Column Selection. Mobile Phase
Selection. Parameters Affecting Retention. Instrumental Aspects
of Supercritical Fluid Chromatography. References. 7. Thin-
Layer Chromatography Introduction. Theoretical
Considerations. Stationary Phases for TLC. Development
Techniques. Mobile Phase Optimization. Quantitative Evaluation
of Thin-Layer Chromatography. References. 8. Sample
Preparation for Chromatographic Analysis Introduction.
Problems in Obtaining a Representative Sample. Isolation and
Concentration Techniques Using Physical Methods. Isolation and
Concentration Techniques Using Solvent Extraction. Sample Cleanup
Using Liquid Chromatography. Sorption Techniques for Trace
Enrichment of Organics in Water. Multidimensional and Multimodal
Sample Fractionation and Trace Enrichment Techniques. Headspace
Sampling. Air Sampling. Derivatization Techniques for Gas
Chromatography. Derivatization Techniques for Liquid
Chromatography. Derivatives for the Chromatographic Separation
of Inorganic Anions and Cations. Visualization Techniques for
Thin-Layer Chromatography. Qualitative Identification and
Microreaction Techniques for Gas Chromatography. Separation of
Stereoisomers. Pyrolysis Gas Chromatography. References. 9.
Hyphenated Methods for Identification after Chromatographic
Separation Introduction. Instrumental Requirements for Mass
Spectrometry. Interface Requirements for Mass Spectrometry.
Interface Requirements for Chromatographic Sample Introduction
Systems in Mass Spectrometry. Data Management and Quantitative
Ion Monitoring in Mass Spectrometry. Instrumental Requirements
for Chromatographic Sample Introduction Systems in Fourier
Transform Infrared Spectroscopy. Liquid Chromatography/Nuclear
Magnetic Resonance Spectroscopy. References. Subject Index.
- Language: English
- Copyright: © Elsevier Science 1991
- Published: May 29, 1991
- Imprint: Elsevier Science
- eBook ISBN: 9780444596192
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