Chromatography Today

Chromatography Today

5th Edition - May 29, 1991

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  • Authors: C.F. Poole, S.K. Poole
  • eBook ISBN: 9780444596192

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Description

Chromatography Today provides a comprehensive coverage of various separation methods: gas, liquid, thin-layer, and supercritical fluid-chromatography, and capillary electrophoresis. Particular attention is paid to the optimization of these techniques in terms of kinetic parameters and retention mechanisms. When these facts are understood, method selection and optimization becomes a more logical process. Sample preparation methods are treated fully as they frequently represent an integral part of the total analytical method. Also described are preparative-scale separations used for isolating significant amounts of product which are generally achieved under conditions that are not identical to those used for analytical separations. The most common hyphenated methods used for sample identification are discussed from the perspective of the information they yield and the requirements of common interfaces. The scope and level of discussion are designed to be appropriate for various user groups. This book should be suitable for use as a graduate-level student textbook in separation science, a text for professional institutes offering short courses in chromatography, and as a self-study guide for chromatographers to refresh their knowledge of the latest developments in the field. The book is extensively illustrated with over 200 figures, 110 tables and 3,300 references, largely to the contemporary literature.

Table of Contents

  • 1. Fundamental Relationships of Chromatography
    Introduction. Retention. Flow in Porous Media. Band Broadening
    Mechanism. Peak Shape Models. Parameters Affecting Resolution.
    Optimization of Kinetic Column Variables. Principles of
    Quantitation in Column Chromatography. References. 2. The
    Column in Gas Chromatography
    Introduction. Packed Column
    Gas-Liquid Chromatography. Open Tubular Columns. Evaluation of
    the Quality of Open Tubular Columns. Retention in Gas-Liquid
    Chromatography. Gas-Solid Chromatography. Preparative-Scale Gas
    Chromatography. References. 3. Instrumental Aspects of Gas
    Chromatography
    Introduction. Pneumatic Systems. Thermal
    Zones. Sample Inlets. Detection Devices for Gas Chromatography.
    Column Connectors and Effluent Splitters. References. 4 The
    Column in Liquid Chromatography
    Introduction. Column Packing
    Materials. Column Preparation. Column Evaluation and Test
    Methods. Retention Mechanisms in Liquid Chromatography. Method
    Development Strategies for Liquid Chromatography. Preparative-
    Scale Liquid Chromatography. Capillary Electrophoretic Separation
    Methods. References. 5. Instrumental Aspects of High Pressure
    Liquid Chromatography
    Introduction. Requirements with Respect
    to Extracolumn Dispersion. Solvent Reservoirs and Solvent
    Degassing. Solvent Delivery Systems. Injection Devices.
    Detectors. References. 6. Supercritical Fluid
    Chromatography
    Introduction. Column Selection. Mobile Phase
    Selection. Parameters Affecting Retention. Instrumental Aspects
    of Supercritical Fluid Chromatography. References. 7. Thin-
    Layer Chromatography
    Introduction. Theoretical
    Considerations. Stationary Phases for TLC. Development
    Techniques. Mobile Phase Optimization. Quantitative Evaluation
    of Thin-Layer Chromatography. References. 8. Sample
    Preparation for Chromatographic Analysis
    Introduction.
    Problems in Obtaining a Representative Sample. Isolation and
    Concentration Techniques Using Physical Methods. Isolation and
    Concentration Techniques Using Solvent Extraction. Sample Cleanup
    Using Liquid Chromatography. Sorption Techniques for Trace
    Enrichment of Organics in Water. Multidimensional and Multimodal
    Sample Fractionation and Trace Enrichment Techniques. Headspace
    Sampling. Air Sampling. Derivatization Techniques for Gas
    Chromatography. Derivatization Techniques for Liquid
    Chromatography. Derivatives for the Chromatographic Separation
    of Inorganic Anions and Cations. Visualization Techniques for
    Thin-Layer Chromatography. Qualitative Identification and
    Microreaction Techniques for Gas Chromatography. Separation of
    Stereoisomers. Pyrolysis Gas Chromatography. References. 9.
    Hyphenated Methods for Identification after Chromatographic
    Separation
    Introduction. Instrumental Requirements for Mass
    Spectrometry. Interface Requirements for Mass Spectrometry.
    Interface Requirements for Chromatographic Sample Introduction
    Systems in Mass Spectrometry. Data Management and Quantitative
    Ion Monitoring in Mass Spectrometry. Instrumental Requirements
    for Chromatographic Sample Introduction Systems in Fourier
    Transform Infrared Spectroscopy. Liquid Chromatography/Nuclear
    Magnetic Resonance Spectroscopy. References. Subject Index.

Product details

  • Language: English
  • Copyright: © Elsevier Science 1991
  • Published: May 29, 1991
  • Imprint: Elsevier Science
  • eBook ISBN: 9780444596192

About the Authors

C.F. Poole

S.K. Poole

Affiliations and Expertise

Wayne State University, Detroit, MI, USA

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