Petroleum mixtures consist primarily of relatively unreactive complex hydrocarbons covering a wide boiling range. Such mixtures are difficult to separate by most analytical techniques. Therefore, the petroleum industry has for many years played a leading role in the development of chromatographic methods of analysis. Since the last book specifically concerned with chromatographic analysis of petroleum appeared 15 years ago, numerous advances have been made including developments in liquid and supercritical fluid chromatography, the advent of silica capillary columns with bonded stationary phases and the commercial availability of new selective detectors.
The current book contains chapters written by experts concerning the analysis of mixtures ranging from low boiling gases to waxes and crude oils. Silica capillary columns offer excellent resolution but they cannot separate all mixtures; therefore a chapter is devoted to the powerful complementary technique of multidimensional gas chromatography. The analysis of polymers by hydrodynamic chromatography is described as is the analysis of aqueous ionic mixtures by capillary electrophoresis. The atomic emission detector, the oxygen FID and the sulfur chemiluminescence detectors are described and a chapter is devoted to data handling.
Although the volume is specifically aimed at the petroleum analyst, there is much information of general interest which should be of benefit to a very wide readership.
- The analysis of hydrocarbon gases (C.J. Cowper). 2. Advances in simulated distillation (D.J. Abbott). 3. The chromatographic analysis of refined and synthetic waxes (A. Barker). 4. Hydrodynamic chromatography of polymers (J. Bos, R. Tijssen). 5. Chromatography in petroleum geochemistry (S.J. Rowland, A.T. Revill). 6. The O-FID and its applications in petroleum product analysis (A. Sironi, G.R. Verga). 7. Microwave plasma detectors (A. de Wit, J. Beens). 8. The sulfur chemiluminescence detector (R.S. Hutte). 9. Multi-column systems in gas chromatography (H. Mahler, T. Maurer, F. Müller). 10. Supercritical fluid extraction (T.P. Lynch). 11. Supercritical fluid chromatography (I. Roberts). 12. HPLC and column liquid chromatography (A.C. Neal). 13. Modern data handling methods (N. Dyson). 14. Capillary electrophoresis in the petroleum industry (T. Jones, G. Bondoux).
- © Elsevier Science 1995
- 24th November 1994
- Elsevier Science
- eBook ISBN:
- Hardcover ISBN:
Burton, South Wirral, UK
@qu:This excellent book can be read with profit by all chromatographers, and should become a standard reference work for the petroleum analyst. ...there is enough highly interesting and well-described material in this book for it to belong on the shelf of every petroleum analyst. @source:Analytical Chemistry @qu:...well referenced and indexed... a good, up-to-date source of information @source:Chromatographia @qu:...manages to fill a gap. It will provide a good reference source for those involved in the analysis of petroleum products. @source:The Analyst @qu:...a pleasing consistency of presentation. Author and subject indexes are comprehensive, and the literature is covered through 1993. ...enough highly interesting and well-described material in this book for it to belong on the shelf of every petroleum analyst. @source:Analytical Chemistry @qu:I thoroughly recommend this volume as a valuable reference source and guidebook both to practitioners in the oil industry and to academic researchers in petroleum science using chromatographic techniques. @source:Trends in Analytical Chemistry @qu:Anyone interested in any type of analytical applications in petroleum products will find this book the information needed. @source:Analusis