
Chemistry: Inorganic Qualitative Analysis in the Laboratory
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Chemistry: Inorganic Qualitative Analysis in the Laboratory is a textbook dealing with qualitative analysis in the laboratory, as well as with the process of anion and cation analysis. The book presents an overview of the subject of inorganic qualitative analysis, including as the equipment, reagents, and procedures that are going to be used in the laboratory. Preliminary experiments include the classification of precipitates, handling precipitates, separation techniques, flame tests, Brown ring test, solvent extraction. The text also describes in detail how to prepare the experiment for anion and cation analysis such as testing for water solubility in a solid sample or the sodium carbonate treatment of a water-soluble sample. The book also explains the qualitative analysis for anions in preliminary and specific tests. In the qualitative analysis for cations, the student follows different procedures for Cation Groups I, II, III, IV or V. For example, the ions of Cation Group V cannot be precipitated by any Cation Groups I-IV reagents, nor by any single group reagent. The textbook is suitable for both chemistry teachers and freshmen students.
Table of Contents
To the Instructor
Chapter 1 Introduction to Qualitative Analysis in the Laboratory
1.1 An Overview of Inorganic Qualitative Analysis
1.2 Definitions of Terms Used in Qualitative Analysis
Chapter 2 Equipment, Reagents, and Procedures
2.1 The Semimicro Scale
2.2 Basic Glassware
Cleaning Glassware
Stirring Rods
Droppers and Pipets
Wash Bottles
2.3 Reagents
2.4 Handling Solutions and Reagents
Measuring and Transferring Solutions and Reagents
Diluting and Mixing Solutions and Reagents
Heating Solutions
Evaporating Solutions
Testing Solutions
2.5 Handling Precipitates
Precipitation
Separating Precipitates by Centrifugation
Washing and Transferring Precipitates after Centrifugation
Separating Precipitates by Filtration
Washing and Transferring Precipitates after Filtration
Sulfide Precipitations
2.6 Flame Tests
2.7 Laboratory Safety
General Safety Precautions
Avoiding Burns
Avoiding Cuts
Avoiding Chemical Accidents
Chapter 3 Laboratory Records and Preliminary Experiments
3.1 Making and Recording Observations
3.2 The Laboratory Notebook
3.3 The Laboratory Report
3.4 Preliminary Experiments
Experiment 1. Classification of Precipitates
Experiment 2. Handling Precipitates
Experiment 3. Separation Techniques
Experiment 4. Flame Tests
Experiment 5. Volatization
Experiment 6. Brown Ring Test
Experiment 7. Solvent Extraction
Prelaboratory Questions
Laboratory Report
Chapter 4 Preparations for Anion and Cation Analysis
4.1 Reading the Written Procedures
4.2 Preparing a Sample for Anion or Cation Analysis
General Solubility Considerations
Samples for Anion Analysis
Samples for Cation Analysis
Dissolution of Alloys
Chapter 5 Qualitative Analysis for Anions
5.1 Anions: The Preliminary Tests
5.2 Anions: The Specific Tests
Prelaboratory Questions
Laboratory Report
Chapter 6 Qualitative Analysis for Cations
6.1 Procedures for Analysis of Cation Group 1
Prelaboratory Questions
Laboratory Report
6.2 Procedures for Analysis of Cation Group II
Prelaboratory Questions
Laboratory Report
6.3 Procedures for Analysis of Cation Group III
Prelaboratory Questions
Laboratory Report
6.4 Procedures for Analysis of Cation Group IV
Prelaboratory Questions
Laboratory Report
6.5 Procedures for Analysis of Cation Group V
Prelaboratory Questions
Laboratory Report
Laboratory Reports for Unknowns and Alloy Analysis
Appendix List of Equipment
Product details
- No. of pages: 138
- Language: English
- Copyright: © Academic Press 1980
- Published: September 15, 1980
- Imprint: Academic Press
- eBook ISBN: 9780323161046
About the Author
Clyde Metz
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