Applications of Polymer Spectroscopy - 1st Edition - ISBN: 9780121254506, 9780323137959

Applications of Polymer Spectroscopy

1st Edition

Authors: E.G. Brame
eBook ISBN: 9780323137959
Imprint: Academic Press
Published Date: 28th September 1978
Page Count: 300
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Description

Applications of Polymer Spectroscopy focuses on the use of spectroscopy for the determination of polymer structure. This book is divided into three general areas of spectroscopy: nuclear magnetic resonance (NMR) spectroscopy, infrared spectroscopy, and mass spectroscopy. This text is comprised of 16 chapters and begins with a discussion on the applications of NMR spectroscopy, including carbon-13 NMR, proton NMR, and fluorine-19 NMR. The next section considers infrared spectroscopy, with special consideration to the Fourier transform method and the dynamic method of handling the examination of polymer films. The book then examines the applications of mass spectroscopy, which include the usual characterization of decomposition products both by direct and indirect means and by stressing the polymer. The use of chemiluminescence, Raman spectroscopy, and electron spin resonance methods is also covered. The last chapter describes the mass spectrometry of thermally treated polymers. This book is a valuable resource for scientists, students, and researchers in fields ranging from polymer science and materials science to chemistry and engineering.

Table of Contents


List of Contributors

Preface

1 Fluorine-19 and Carbon-13 NMR Spectra of Polyperfluorobutadiene

I. Introduction

II. Experimental Technique

III. Results and Discussion

References

2 Carbon-13 NMR Spectra of Polyalkenamers

I. Introduction

II. Experimental Technique

III. Results

IV. Discussion

References

3 Proton and Carbon-13 NMR Spectra of Ethylene-Carbon Monoxide Copolymers

I. Introduction

II. Experimental Technique

III. Results and Discussion

Appendix. Sequence Distributions in Semialternating Copolymers

References

4 Instrumental Characterization of Ethylene-Ethyl Acrylate-Carbon Monoxide Terpolymers

I. Introduction

II. Experimental Technique

III. Compositional Analysis and Sequence Distribution by Proton Magnetic Resonance (PMR)

IV. Analysis by Infrared

V. Analysis by Differential Scanning Calorimetry (DSC)

VI. Conclusions

Appendix. PMR Calculation of Terpolymer Content—Ethylene-Ethyl Acrylate-Carbon Monoxide Terpolymers

References

5 Carbon-13 Spin Relaxation Parameters of Bulk Synthetic Polymers

I. Introduction

II. Totally Amorphous Polymers

III. Chemical Structure and Segmental Motion

IV. Semicrystalline Polymers

References

6 NMR and Infrared Study of Thermal Oxidation of cis 1,4-Polybutadiene

I. Introduction

II. Experimental Technique

III. Results

IV. Discussion

V. Summary

References

7 NMR and Infrared Study of Photosensitized Oxidation of Polyisoprene

I. Introduction

II. Experimental Technique

III. Results and Discussion

IV. Kinetics of Singlet Oxygenation

V. Summary

References

8 Chemiluminescence Study of the Autoxidation of cis-1,4-Polyisoprene

I. Introduction

II. Experimental Technique

III. Results

IV. Discussion

References

9 Raman Spectra of Biopolymers

I. Introduction

II. Experimental Technique

III. Applications

References

10 Fourier Transform Infrared Spectra of Macromolecules

I. Introduction

II. Optically Dense Materials

III. Spectral Manipulations

References

11 Reflection-Absorption Infrared Spectra of γ-Aminopropyltriethoxysilane Adsorbed on Bulk Iron

I. Introduction

II. Reflection-Absorption Infrared Spectroscopy

III. Experimental Technique

IV. Results and Discussion

V. Conclusions

References

12 Dynamic Infrared of Polymers

I. Introduction

II. Frequency Shifting

III. Molecular Orientation

IV. Applications

V. Conclusions

References

13 Characterization of Polymer Deformation and Fracture

I. Kinetic Models of Polymer Fracture

II. ESR Observations of Stress-Induced Bond Rupture in Polymers

III. Associated Studies

References

14 Stress Mass Spectrometry of Nylon 66

I. Introduction

II. Experimental Technique

III. Results and Discussion

IV. Conclusion

References

15 Characterization of Polymer Decomposition Products by Electron Impact and Chemical Ionization Mass Spectrometry

I. Introduction

II. Mass Spectrometry

III. Applications

IV. Conclusions

References

16 Mass Spectrometry of Thermally Treated Polymers

I. Introduction

II. Instrumentation and Experimental Techniques

III. Results and Discussion

IV. Summary

References

Author Index

Subject Index




Details

No. of pages:
300
Language:
English
Copyright:
© Academic Press 1978
Published:
Imprint:
Academic Press
eBook ISBN:
9780323137959

About the Author

E.G. Brame