Annual Reports on NMR Spectroscopy - 1st Edition - ISBN: 9780128021248, 9780128023327

Annual Reports on NMR Spectroscopy, Volume 84

1st Edition

Serial Editors: Graham Webb
eBook ISBN: 9780128023327
Hardcover ISBN: 9780128021248
Imprint: Academic Press
Published Date: 23rd February 2015
Page Count: 310
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Table of Contents

  • Preface
  • Chapter One: Applications of 1H–15N Long-Range Heteronuclear Shift Correlation and 15N NMR in Alkaloid Chemistry
    • Abstract
    • 1 Introduction
    • 2 Previous Reviews
    • 3 Experiments and Parametric Considerations
    • 4 Computer-Assisted Structure Elucidation—The Impact of 15N Data
    • 5 Covariance Calculation of 13C–15N Heteronuclear Shift Correlation Spectra
    • 6 Applications of Long-Range 1H–15N Heteronuclear Shift Correlation to Alkaloids not Previously Reviewed
    • 7 Applications of Long-Range 1H–15N Heteronuclear Shift Correlation to Alkaloids
    • 8 Miscellaneous Alkaloid Structures
    • 9 Alkaloid Structures Revised with the Aid of 1H–15N HMBC Data
    • 10 Conclusions
  • Chapter Two: Solid-State Covariance NMR Spectroscopy
    • Abstract
    • 1 Introduction
    • 2 Overview of Covariance NMR Spectroscopy
    • 3 Applications of Solid-State Covariance NMR Spectroscopy
    • 4 Improvement of Covariance Toward Further Time Saving
    • 5 Variants of Solid-State Covariance NMR Spectroscopy
    • 6 Summary
    • Acknowledgments
  • Chapter Three: Recent Advances in Chlorine, Bromine, and Iodine Solid-State NMR Spectroscopy
    • Abstract
    • 1 Introduction
    • 2 Theory and Modeling
    • 3 Solid-State Chlorine-35/37 Nuclear Magnetic Resonance
    • 4 Solid-State Bromine-79/81 Nuclear Magnetic Resonance
    • 5 Solid-State Iodine-127 Nuclear Magnetic Resonance
    • 6 Concluding Remarks
    • Acknowledgments
  • Chapter Four: Recent Advances in Small Molecule NMR: Improved HSQC and HSQMBC Experiments
    • Abstract
    • 1 Introduction
    • 2 The Basic HSQC Experiment
    • 3 Speeding-Up HSQC Data Acquisition
    • 4 High-Resolved HSQC Using Pure Shift NMR
    • 5 HSQC Methods for Measuring 1J(CH)
    • 6 HSQMBC Experiments for Measuring nJ(CH)
    • 7 Other Methods
    • 8 Conclusion
    • Acknowledgments
  • Chapter Five: A Review of 91Zr Solid-State Nuclear Magnetic Resonance Spectroscopy
    • Abstract
    • 1 Introduction
    • 2 Experimental Methods
    • 3 Chronological Literature Review
    • 4 Conclusions and Future Outlook
    • Acknowledgments
  • Subject Index

Description

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.

Key Features

  • This volume of Annual Reports on NMR Spectroscopy focuses on the analytical tools used by chemists and physicists, taken together with other volumes of this series, an excellent account of progress in NMR and its many applications is provided and anyone using NMR will find interest in this Serial

Readership

Organic, inorganic, analytical and physical chemists, biochemists, structural biologists, physicists and all those studying and using NMR spectroscopy


Details

No. of pages:
310
Language:
English
Copyright:
© Academic Press 2015
Published:
Imprint:
Academic Press
eBook ISBN:
9780128023327
Hardcover ISBN:
9780128021248

Reviews

"An eclectic and timely collection of reviews on recent advances and hot topics in nuclear magnetic resonance spectroscopy. ...faithful in citing seminal literature and past reviews, while including most, if not all, recent work in the past 10 years. For those who have an interest in NMR spectroscopy, this book would be an excellent resource." --Journal of the American Chemical Society


About the Serial Editors

Graham Webb Serial Editor

Editor of about 150 volumes, mostly dealing with aspects of NMR. Retired Professor of Chemistry from the University of Surrey.

Affiliations and Expertise

Royal Society of Chemistry, Burlington House, London, UK