Annual Reports on NMR Spectroscopy

Annual Reports on NMR Spectroscopy

1st Edition - July 1, 2013

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  • Editor: Graham Webb
  • Hardcover ISBN: 9780124080973
  • eBook ISBN: 9780124079045

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Description

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.

Key Features

  • This volume of Annual Reports on NMR Spectroscopy focuses on the analytical tool used by chemists and physicists and inlcudes topics such as Profiling of Food Samples, Recent Advances in Solution NMR Studies and Magic Angle Spinning NMR Studies of Protein Assemblies

Readership

Organic, inorganic, analytical and physical chemists, biochemists, structural biologists, physicists and all those studying and using NMR spectroscopy.

Table of Contents

  • Contributors

    Preface

    Chapter One. NMR Studies of Crown Ether–Cyclodextrin Complexes

    Abstract

    1 Introduction

    2 Cyclodextrins: The Molecular Containers

    3 Crown Ethers and Cryptands: The Beginning of Supramolecular Chemistry

    4 Cyclodextrin–Crown Ether Complexes: Non-NMR Studies

    5 Cyclodextrin–Crown Ether Interactions: An NMR Look

    6 Complexes of Cyclam Derivatives

    7 Conclusions

    References

    Chapter Two. 15N and 31P NMR Coordination Shifts in Transition Metal Complexes with Nitrogen- and Phosphorus-Containing Heterocycles

    Abstract

    1 Transition Metal Complexes with Azines

    2 Transition Metal Complexes with Azoles

    3 Transition Metal Complexes with Purines

    4 Transition Metal Complexes with 1,2,4-Triazolo-[1,5a]-Pyrimidines

    5 Transition Metal Complexes with Phosphinines

    6 Transition Metal Complexes with Phospholes

    7 Conclusions

    References

    Chapter Three. Quantification of Complex Mixtures by NMR

    Abstract

    1 Introduction

    2 Practical Background

    3 NMR Acquisition Methods

    4 Post-Acquisition NMR Processing

    5 Application Areas of qNMR

    6 Future Developments

    Acknowledgements

    References

    Chapter Four. Proton NMR Profiling of Food Samples

    Abstract

    1 Introduction

    2 Sample Preparation

    3 NMR Techniques

    4 Data Treatment

    5 Statistical Analysis

    6 Applications

    References

    Chapter Five. Magic Angle Spinning NMR Studies of Protein Assemblies: Recent Advances in Methodology and Applications

    Abstract

    1 Introduction

    2 Recent Methodological Advances for MAS NMR Studies of Protein Assemblies

    3 Recent MAS NMR Applications to Study Protein Assemblies

    4 Conclusions and Outlook

    References

    Chapter Six. Recent Advances in Solution NMR Studies: 13C Direct Detection for Biomolecular NMR Applications

    Abstract

    1 Introduction

    2 Intrinsic Properties of Heteronuclei (13C, 15N)

    3 Examples of Applications

    References

    Index

Product details

  • No. of pages: 448
  • Language: English
  • Copyright: © Academic Press 2013
  • Published: July 1, 2013
  • Imprint: Academic Press
  • Hardcover ISBN: 9780124080973
  • eBook ISBN: 9780124079045

About the Editor

Graham Webb

Editor of about 150 volumes, mostly dealing with aspects of NMR. Retired Professor of Chemistry from the University of Surrey.

Affiliations and Expertise

Royal Society of Chemistry, Burlington House, London, UK

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