Analytical Sample Preparation With Nano- and Other High-Performance Materials

Analytical Sample Preparation With Nano- and Other High-Performance Materials

1st Edition - October 22, 2021

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  • Editors: Rafael Lucena, M. Soledad Cardenas Aranzana
  • eBook ISBN: 9780128221723
  • Paperback ISBN: 9780128221396

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Description

Analytical Sample Preparation With Nano- and Other High-Performance Materials covers advanced sample treatment techniques and the new materials that can be used to boost their performance. The evolution of sample treatment over the last two decades has resulted in the development of new techniques and application of new materials. This is a must-have resource for those studying advanced analytical techniques and the role of high-performance materials in analytical chemistry. The book explains the underlying principles needed to properly understand sample preparation, and also examines the latest materials - including nanomaterials - that result in greater sensitivity and specificity. The book begins with a section devoted to all the various sample preparation techniques and then continues with sections on high-performance sorbents and high-performance solvents.

Key Features

  • Combines basic, fundamental principles and advanced concepts and applications for a comprehensive treatment of sample preparation with new materials
  • Defines nano- and other high-performance materials in this context, including carbon nanoparticles, inorganic nanoparticles, ionic liquids, supramolecular solvents, and more
  • Includes discussion of all the latest advancements and new findings in both techniques and materials used for proper sample preparation

Readership

Students learning advanced analytical techniques and the role of high-performance materials in analytical chemistry; researchers in the Analytical Chemistry field

Table of Contents

  • Cover image
  • Title page
  • Table of Contents
  • Copyright
  • List of contributors
  • Preface by Rafael Lucena
  • Preface by Elefteria Psillakis
  • 1. Analytical sample treatment: basics and trends
  • Abstract
  • 1.1 Introduction to analytical sample preparation
  • 1.2 Fundament and classification
  • 1.3 Main trends in the field
  • Acknowledgments
  • References
  • 2. Miniaturized solid-phase extraction
  • Abstract
  • 2.1 Introduction
  • 2.2 Confined micro-solid phase extraction
  • 2.3 Dispersive micro-solid phase extraction
  • 2.4 Conclusions
  • Acknowledgments
  • References
  • 3. Solid-phase microextraction
  • Abstract
  • 3.1 Introduction
  • 3.2 In-fiber and in-tube solid-phase microextraction
  • 3.3 Thin-film microextraction
  • 3.4 Stir-assisted solid-phase microextraction
  • 3.5 Conclusions
  • Acknowledgments
  • References
  • 4. Unconfined liquid-phase microextraction
  • Abstract
  • 4.1 Introduction
  • 4.2 Single-drop microextraction
  • 4.3 Dispersive-based liquid-phase microextraction
  • 4.4 Conclusion
  • Acknowledgments
  • References
  • 5. Analytical microextraction with supported liquid membranes
  • Abstract
  • 5.1 Introduction
  • 5.2 Two-phase hollow-fiber liquid-phase microextraction
  • 5.3 Three-phase hollow-fiber liquid-phase microextraction
  • 5.4 96-Well liquid-phase microextraction
  • 5.5 Solvent bar microextraction
  • 5.6 Electromembrane extraction
  • 5.7 Outlook
  • References
  • 6. Solid–liquid extraction techniques
  • Abstract
  • 6.1 Introduction
  • 6.2 General aspects on SLE
  • 6.3 Classical SLE processes
  • 6.4 Superheated solvent extraction
  • 6.5 Ultrasound-assisted extraction
  • 6.6 Microwaves-assisted extraction
  • 6.7 Comparison and applicability of SHSE, USAE, and MAE
  • 6.8 Conclusions
  • References
  • 7. Microextraction-based samplers for liquid and tissue analysis
  • Abstract
  • 7.1 Introduction
  • 7.2 Microextraction devices for convenient integration of sampling and extraction for liquid and tissues
  • 7.3 Applications
  • 7.4 Conclusion
  • List of Abbreviations
  • References
  • 8. Direct coupling of microextraction with instrumental techniques
  • Abstract
  • 8.1 Introduction
  • 8.2 Coupling of microextraction with spectroscopic techniques
  • 8.3 Coupling of microextraction with mass spectrometry
  • 8.4 Overview of interfaces based on flow analysis, microfluidics, and 3D printing
  • 8.5 Conclusion
  • Acknowledgments
  • References
  • 9. Membrane sorptive phases
  • Abstract
  • 9.1 Introduction
  • 9.2 Polymeric membranes
  • 9.3 Fabric phases
  • 9.4 Paper-based sorptive phases
  • 9.5 Conclusions
  • Acknowledgments
  • References
  • 10. Selectivity-enhanced sorbents
  • Abstract
  • 10.1 Introduction
  • 10.2 Molecularly imprinted polymers
  • 10.3 Restricted access materials
  • 10.4 Selective biosorbents
  • 10.5 Conclusions
  • Acknowledgments
  • References
  • 11. Carbon nanoparticles
  • Abstract
  • 11.1 Introduction
  • 11.2 Carbon-based nanomaterials in sample preparation
  • 11.3 Conclusions
  • Acknowledgments
  • References
  • 12. Metal and metal oxide nanomaterials in sample preparation
  • Abstract
  • 12.1 Introduction
  • 12.2 MNs in sample preparation
  • 12.3 MONs in sample preparation
  • 12.4 Application of MONs in sample preparation
  • 12.5 Conclusions
  • References
  • 13. Reticular materials in sorbent-based extraction methods
  • Abstract
  • 13.1 Introduction
  • 13.2 Incorporation of reticular materials in analytical sample preparation methods
  • 13.3 Concluding remarks
  • Acknowledgments
  • List of abbreviations
  • References
  • 14. Polymeric nanocomposites
  • Abstract
  • 14.1 Introduction
  • 14.2 Magnetic polymeric nanocomposites
  • 14.3 Carbon-based nanocomposites
  • 14.4 Metal-based polymeric nanocomposites
  • 14.5 Conclusions
  • Acknowledgments
  • List of abbreviations
  • References
  • 15. Monolithic solids: synthesis and uses in microextraction techniques
  • Abstract
  • 15.1 Introduction
  • 15.2 Preparation of monolithic beds
  • 15.3 Applications of monolithic materials in microextraction techniques
  • 15.4 Conclusions and future perspectives
  • Acknowledgments
  • List of abbreviations
  • References
  • 16. Ionic liquids
  • Abstract
  • 16.1 Conventional ionic liquids
  • 16.2 Magnetic ionic liquids
  • 16.3 Polymeric ionic liquids
  • 16.4 Conclusion
  • Acknowledgments
  • References
  • 17. Switchable solvents
  • Abstract
  • 17.1 Introduction
  • 17.2 Applications of switchable solvents in sample preparation
  • 17.3 Concluding remarks
  • Acknowledgments
  • References
  • 18. Deep eutectic solvents in microextraction
  • Abstract
  • 18.1 Introduction
  • 18.2 Synthesis and physicochemical properties of DES
  • 18.3 Classification and types of DES
  • 18.4 Use of DES in microextraction
  • 18.5 Factors affecting extraction efficiency with DES
  • 18.6 Trends in DES-based microextractions
  • 18.7 Conclusions and future perspectives
  • References
  • 19. Supramolecular solvents in microextraction techniques
  • Abstract
  • 19.1 Introduction
  • 19.2 Supramolecular solvent formation
  • 19.3 Supramolecular solvent properties relevant for microextraction
  • 19.4 Microextraction formats
  • 19.5 Concentration factors
  • 19.6 Compatibility of supramolecular solvent with separation and detection techniques
  • 19.7 Analytical applications
  • 19.8 Conclusion
  • Acknowledgments
  • References
  • Index

Product details

  • No. of pages: 560
  • Language: English
  • Copyright: © Elsevier 2021
  • Published: October 22, 2021
  • Imprint: Elsevier
  • eBook ISBN: 9780128221723
  • Paperback ISBN: 9780128221396

About the Editors

Rafael Lucena

Prof. Dr. Rafael Lucena has been a professor of Analytical Chemistry since 2010. He has coauthored more than 100 scientific articles on different analytical aspects, with microextraction techniques being the core of his research. He co-edited a special volume in the journal Analytical and Bioanalytical Chemistry and an e-book on the topic. In addition, he is editing a blog (Microextraction Tech) focused on sample treatment techniques. Rafael has directed 8 Ph.D. theses and several master and degree theses. He is the secretary of the Research Institute of Fine Chemistry and Nanochemistry, an organization involving more than 125 researchers in different areas of chemistry. He has also been involved in organizing several meetings such as NANOUCO, a monographic conference on nanochemistry. He also acts as a reviewer in many journals and project evaluator for organizations such as Fondecyt (Chile). He is currently member of the editorial board of Molecules.

Affiliations and Expertise

Associate Professor, Analytical Chemistry, University of Cordoba, Spain

M. Soledad Cardenas Aranzana

Prof. Dr. M. Soledad Cárdenas Aranzana has been a full professor of Analytical Chemistry since 2009. Her research interests comprise microextraction techniques, including developing new approaches, synthesizing novel nanomaterials based on carbon, metallic nanoparticles and polymers. She has co-authored 202 scientific articles and contributed to 16 book chapters and an ebook (Microextraction Analytical Techniques, 2017, Bentham. She has presented 170 conference communications, co-supervised 16 doctoral theses, and participated in 7 contracts and 1 patent. She has acted as regular reviewer of the Spanish National Evaluation and Foresight Agency (ANEP) and external reviewer for the Portuguese Foundation of Science and Technology and the Agencia Nacional de Promoción Científica y Tecnológica (ANPCyT, Argentina). She has also been member of the expert panel for the evaluation of researchers in various national programs. Currently, she is president of the A3 Committee (Chemistry) of the Spanish National Agency for Quality Assessment and Accreditation (ANECA)

Affiliations and Expertise

Full Professor, Analytical Chemistry, University of Córdoba, Spain

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