Analytical Pyrolysis

Analytical Pyrolysis

1st Edition - January 1, 1977

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  • Editor: C.E.R. Jones
  • eBook ISBN: 9780444601407

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Description

Analytical Pyrolysis presents the Proceedings of the Third International Symposium on Analytical Pyrolysis, held in Amsterdam on September 7-9, 1976. It looks at newly emergent techniques in analytical pyrolysis, including pyrolysis mass spectrometry, gas chromatography, thin-layer chromatography, and pyrolysis-gas liquid chromatography. The book also covers topics ranging from automation and microbiology to forensic science and pharmacology, reproducibility and specificity, biochemistry, laser-induced pyrolysis, pyrolytic reaction mechanisms, and polymers. Comprised of 50 chapters, this book begins with a discussion of automatic analysis of tire rubber blends using computer-linked pyrolysis gas chromatography, thermal procedures in coupling with thin-layer chromatography, the role of pyrolysis-gas liquid chromatography in biomedical studies, and the identification of microorganisms by pyrolysis gas-liquid chromatography. It then examines forensic applications of analytical pyrolysis techniques, structure and degradation behavior of synthetic polymers using pyrolysis in combination with field ion mass spectrometry, determination of polysaccharides in fulvic acids by pyrolysis gas chromatography, and application of Curie-point pyrolysis mass spectrometry in fungal taxonomy. The reader is also introduced to pyrolysis mass spectrometry of model compounds labeled with stable isotopes, the use of pyrolysis/gas chromatography to determine the quality of porous polymers of styrene cross-linked with divinyl benzene, and application of pyrohydrolysis for a rapid and accurate determination of halides in silicate rocks and minerals. This volume will benefit students, researchers, chemists, and scientists working in the field of analytical pyrolysis.

Table of Contents


  • Preface

    Automation

    Automatic analysis of tyre rubber blends by computer-linked pyrolysis gas chromatography

    Special techniques

    Pyrolysis field ionization and field desorption mass spectrometry of biomacromolecules, microorganisms, and tissue material

    Thermal procedures in coupling with thin-layer chromatography

    An automated analytical system for complex mixtures utilizing separation by high-resolution mass spectrometry and identification by collisional activation mass spectrometry

    Microbiology

    The role of pyrolysis-gas liquid chromatography in biomedical studies

    Comparison on oral streptococci by pyrolysis

    Pyrolysis gas-liquid chromatography studies of the genus Bacillus . Effect of growth time on pyrochromatogram reproducibility

    The identification of microorganisms by pyrolysis gas-liquid chromatography

    Forensic science and pharmacology

    Forensic applications of analytical pyrolysis techniques

    Application of Curie-point pyrolysis gas chromatography using high-resolution glass open-tubular columns

    The identification of formulated drugs by Py-GC-MS

    Pyrolysis mass spectrometry

    Structure and degradation behaviour of synthetic polymers using pyrolysis in combination with field ion mass spectrometry

    Direct pyrolysis of aromatic and aliphatic polyesters in the mass spectrometer

    Reproducibility and specificity

    Some numerical aspects of reproducibility and specificity

    Soil chemistry and geochemistry

    Pyrolysis studies on humus in freely drained Scottish soils

    The determination of polysaccharides in fulvic acids by pyrolysis gas chromatography

    Pyrolysis as a possible means of determining the petroleum generating potential of sedimentary organic matter

    Curie-point pyrolysis in organic geochemistry

    Biochemistry

    Pyrolysis GLC of biomedically interesting molecules

    The application of Curie-point pyrolysis mass spectrometry in fungal taxonomy

    Laser pyrolysis

    Laser induced pyrolysis techniques

    Laser pyrolysis GC/MS of membrane components

    Reaction mechanisms

    Pyrolytic reaction mechanisms

    Pyrolysis mass spectrometry of model compounds labelled with stable isotopes

    Curie-point pyrolysis as a guide to new syntheses

    Pyrolysis-mass spectrometry of truxillic and truxinic polyamides and related copolyamides

    Polymers

    Pyrolysis/gas chromatography as a means of determining the quality of porous polymers of styrene cross-linked with divinyl benzene

    The analysis of automotive paints by pyrolysis gas chromatography

    Characterisation of textile materials by thermal degradation: A critique of pyrolysis GC and thermogravimetry

    An interfaced vapor phase instrumental system for thermal analysis and pyrolysis

    Analytical pyrolysis of inorganic and thermostable polymers

    Pyrolysis-gas chromatography and spectroscopic identification of fluorine polymers

    Automation of a thermogravimetry apparatus with a laboratory computer

    Microstructures of vinyl-type copolymers by pyrolysis-gas chromatography

    Appendix

    Gas Chromatographic mass spectrometry

    Curie-point evaporation: A new and simple technique for splitless injection on open tubular capillary columns

    The classification and identification of microorganisms by pyrolysis-mass spectrometry

    Quantitative and kinetic studies by pyrolysis gas chromatography

    Curie-point pyrolysis mass spectrometry using a Knudsen reactor

    The scope of automated pyrolysis mass spectrometry

    Pyrolysis gas Chromatographic correlation trials of the American Society for Testing and Materials

    Specificity in analytical pyrolysis

    Study of the thermal degradation of organic polymers using different metal surfaces as the heat source

    Application of pyrohydrolysis for a rapid and accurate determination of halides in silicate rocks and minerals

    The quantitative analysis of choline esters in biological samples by pyrolysis gas chromatography-mass spectrometry

    Laser pyrolysis-gas chromatographic-mass spectrometric analysis of epoxy composites

    Laser pyrolysis/mass spectrometry of biopolymers

    Thermochemistry of polybenzimidazole foams

    Theory of thermal decomposition and volatilization of normal alkanes and linear polyethylene

    Identification and structural investigation of phenolic resins by a novel set of PGC techniques




Product details

  • No. of pages: 434
  • Language: English
  • Copyright: © Elsevier 1977
  • Published: January 1, 1977
  • Imprint: Elsevier
  • eBook ISBN: 9780444601407

About the Editor

C.E.R. Jones

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