Analytical Chemistry of Niobium and Tantalum details the methods in understanding the chemistry of niobium and tantalum, which includes separation, identification, and quantification. The text first discusses the general topics about niobium and tantalum, such as history, metallurgical properties, and applications. Next, the selection covers the properties of niobium and tantalum and their compounds. The subsequent chapters tackle the various analytical chemistry processes that can be applied to niobium and tantalum, such as spectrographic determination; titrimetric methods; and colorimetric determinations. The book will be of great use to chemists, chemical engineers, and metallurgists.
I. Introduction II. Properties of Niobium and its Compounds III. Properties of Tantalum and its Compounds IV. Compounds of Niobium and Tantalum of Analytical Interest V. Detection and Identification VI. Dissolution of the Sample, Precipitation Separations and Gravimetric Determinations VII. Separations by Solvent Extraction VIII. Ion Exchange and Chromatography, Separations and Determinations IX. Colorimetric Determinations with Hydrogen Peroxide X. Colorimetric Determinations with Polyphenols XL Colorimetric Determinations with Thiocyanate XII. Colorimetric Determinations with Other Reagents XIII. Titrimetric Methods XIV. Chlorination and Volatilization in Determinations XV. Polarography of Niobium and Tantalum XVI. X-Ray Diffraction and X-Ray Fluorescence XVII. Radioactive Tracers and Neutron Activation XVIII. Determination of Impurities XIX. Spectrographic Determination of Niobium and Tantalum and Associated Impurities Author Index Subject Index
- No. of pages:
- © Pergamon 1964
- 1st January 1964
- eBook ISBN: