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| SOLVING PROBLEMS WITH NMR SPECTROSCOPY
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By
Atta-ur- Rahman, University of Karachi, Pakistan
Muhammad Choudhary, University of Karachi
Description
Solving Problems with NMR Spectroscopy presents the basic principles and applications of NMR spectroscopy with only as
much math as is necessary. It shows how to solve chemical structures with NMR by giving clear examples and solutions. This text will
enable organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems to work and
the discussion of their solutions and interpretations will help readers becomeproficient in the application of important, modern 1D and
2D NMR techniques to structural studies.
Audience
Senior and graduate chemistry students and organic, medicinal, and pharmaceutical chemists.
Contents
The Basics of Modern NMR Spectroscopy:
What is NMR? Instrumentation. Creating NMR Signals.
Spin-Echo and Polarization
Transfer:
Spin-Echo Formation in Homonuclear and Heteronuclear Systems. Cross-Polarization. Polarization Transfer in Reverse.
The Second Dimension:
Data Acquisition in 2D NMR. Data Processing in 2D NMR. Plotting 2D Spectra.
Nuclear Overhauser
Effect:
nOe and Selective Population Transfer. Relaxation. Mechanism of nOe. Factors Affecting nOe. Some Practical Hints.
Important
2D NMR Experiments:
Homo- and Heteronuclear J-Resolved Spectroscopy. Homonuclear and Heteronuclear Shift-Correlation
Spectroscopy. Two-Dimensional Nuclear Overhauser Spectroscopy. Two-Dimensional Chemical Exchange Spectroscopy. Homonuclear Hartmann-Hahn
Spectroscopy (HOHAHA), or Total Correlation Spectroscopy (TOCSY). Inverse NMR Spectroscopy. Inadequate.
The Third Dimension:
Basic Philosophy. Types and Positions of Peaks in 3D Spectra.
Recent Developments in NMR Spectroscopy:
Selective Pulses
in Modern NMR Spectroscopy. One-Dimensional Experiments Using Soft Pulses. Heteronuclear Selective 1D NMR Experiments. Two-Dimensional
Experiments Using Soft Pulses. Soft Excitation in Two Dimensions. Three-Dimensional Experiments Using Soft Pulses. Field Gradients.
Logical
Protocol for Solving Complex Structural Problems: 3-Hydroxylupanine. (1)
. (+)-Buxalongifolamidine.
(2)
. References.
Subject Index.
| Bibliographic details |
Paperback, 430 pages, publication date: DEC-1995
ISBN-13: 978-0-12-066320-0
ISBN-10: 0-12-066320-1
Imprint: ACADEMIC PRESS
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| Price and Ordering |
Price:
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EUR 57.95
USD 70.95
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030/771
Last update: 4 Sep 2009
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